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Trihexylboron

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Trihexylboron Basic information
Product Name:Trihexylboron
Synonyms:Trihexylboron;Tri-n-hexylborane;Borane, trihexyl-
CAS:1188-92-7
MF:C18H39B
MW:266.31
EINECS:
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Mol File:1188-92-7.mol
Trihexylboron Structure
Trihexylboron Chemical Properties
Safety Information
MSDS Information
Trihexylboron Usage And Synthesis
Purification MethodsTreat the borane with hex-1-ene and 10% anhydrous Et2O for 6hours at gentle reflux under N2, then distil it in a vacuum through an 18inch glass helices-packed column under N2 taking the fraction b 130o/2.1mm to 137o/1.5mm. The distillate may still contain some di-n-hexylborane [Brown & Subba Rao J Am Chem Soc 81 6423 1959, Mirviss J Am Chem Soc 83 3051 1961]. [Beilstein 4 IV 4362.]
Trihexylboron Preparation Products And Raw materials
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