| Company Name: |
Bide Pharmatech Ltd.
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| Tel: |
400-1647117 15221909166 |
| Email: |
product02@bidepharm.com |
| Products Intro: |
Product Name:Methanesulfinyl chloride
CAS:676-85-7
Purity:90% Package:100mg;250mg;1g;
|
| Company Name: |
ATK CHEMICAL COMPANY LIMITED
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| Tel: |
3429815786 13301662590 |
| Email: |
sales@atkchemical.com |
| Products Intro: |
CAS:676-85-7
Purity:98% Package:1G,5G,100G,500g,1kg
|
| Company Name: |
Bide Pharmatech Ltd.
|
| Tel: |
400-6005915 |
| Email: |
sales@picasso-e.com |
| Products Intro: |
Product Name:Methanesulfinyl chloride
CAS:676-85-7
Purity:90% Package:100mg;250mg;1g
|
|
| | Methanesulfinylchloride Basic information |
| Product Name: | Methanesulfinylchloride | | Synonyms: | Methanesulfinylchloride;methylsulphinyl chloride;Methanesulfinyl chloride (6CI,7CI,8CI,9CI);Methanesulfinic Chloride | | CAS: | 676-85-7 | | MF: | CH3ClOS | | MW: | 98.55 | | EINECS: | | | Product Categories: | | | Mol File: | 676-85-7.mol |  |
| | Methanesulfinylchloride Chemical Properties |
| Boiling point | 55-59 °C(Press: 40 Torr) | | density | 1.494±0.06 g/cm3(Predicted) |
| | Methanesulfinylchloride Usage And Synthesis |
| Synthesis Reference(s) | The Journal of Organic Chemistry, 33, p. 2104, 1968 DOI: 10.1021/jo01269a088
Synthetic Communications, 24, p. 1207, 1994 DOI: 10.1080/00397919408011719 | | Synthesis | A mixture of 23.5 g (0.25 mol) of freshly distilled dimethyl disulfide and 51 g (0.5 mol) of acetic anhydride is chlorinated at -10 to 0℃. During the course of the reaction the color changes from yellow to red and then disappears, at which point the addition of chlorine is suspended, leading to 126 g of reaction mixture. This is distilled in a 45 cm Vigreux column at 2 kPa with cooling. Acetyl chloride distills at 0℃, and at 47–48℃ the almost colorless methanesulfinyl chloride is obtained in 83–86% yield. |
| | Methanesulfinylchloride Preparation Products And Raw materials |
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