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4-Iodoanisole

4-Iodoanisole structure

CAS No.: 696-62-8

Chemical Name:: 4-Iodoanisole

Synonyms: 1-IODO-4-METHOXYBENZENE;P-IODOANISOLE;4-IODOANISOL;Isoform;4-IODANISOLE;p-iodoanisol;4-lodoanisole;4-METHOXYIODOBENZENE;CREM-α;4-iodoether

CBNumber:: CB6450614

Molecular Formula:: C7H7IO

Molecular Weight:: 234.03

MDL Number:: MFCD00001056

MOL File:: 696-62-8.mol

MSDS File:: SDS

Last updated:2023-12-24 16:54:11

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4-Iodoanisole Properties

Melting point	50-53 °C(lit.)
Boiling point	237 °C726 mm Hg(lit.)
Density	1.7904 (estimate)
Flash point	>230 °F
storage temp.	Keep in dark place,Sealed in dry,Room Temperature
solubility	Soluble in ethanol, ether, chloroform.
form	Crystalline Powder and Chunks
color	Off-white to brown
Sensitive	Light Sensitive
BRN	1906692
InChIKey	SYSZENVIJHPFNL-UHFFFAOYSA-N
CAS DataBase Reference	696-62-8(CAS DataBase Reference)
NIST Chemistry Reference	Benzene, 1-iodo-4-methoxy-(696-62-8)
EPA Substance Registry System	Benzene, 1-iodo-4-methoxy- (696-62-8)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H315-H319-H335

Precautionary statements

P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313-P261-P280a-P304+P340-P305+P351+P338-P405-P501a

Hazard Codes

Xi,Xn

Risk Statements

36/37/38

Safety Statements

26-36-24/25

WGK Germany

TSCA

Yes

HS Code

29093090

NFPA 704

	0
1		0

4-Iodoanisole price More Price(42)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	I7608	4-Iodoanisole 98%	696-62-8	25g	$46.8	2024-03-01	Buy
Sigma-Aldrich	I7608	4-Iodoanisole 98%	696-62-8	100g	$140	2024-03-01	Buy
TCI Chemical	I0378	4-Iodoanisole >99.0%(GC)	696-62-8	25g	$30	2024-03-01	Buy
TCI Chemical	I0378	4-Iodoanisole >99.0%(GC)	696-62-8	100g	$82	2024-03-01	Buy
Alfa Aesar	A12144	4-Iodoanisole, 98+%	696-62-8	25g	$34.1	2024-03-01	Buy

Product number	Packaging	Price	Buy
I7608	25g	$46.8	Buy
I7608	100g	$140	Buy
I0378	25g	$30	Buy
I0378	100g	$82	Buy
A12144	25g	$34.1	Buy

4-Iodoanisole Chemical Properties,Uses,Production

Description

4-Iodoanisole (chemical formula: C7H7IO) is an organic compound being soluble in ethanol, ether and chloroform. It has a wide range of medicals industrial applications. For example, it can be used as human and animal nutrition products, antiseptics, disinfectants, pharmaceutical intermediates, polarizing films for liquid crystal display (LCD) chemicals. Its iodine derivatives can also be used as organic building blocks and analytic reagents.

References

https://www.fishersci.pt/shop/products/4-iodoanisole-98-7/11480113

Chemical Properties

off-white to brown crystalline powder and chunks. Melting point 51-52 ℃, boiling point 237 ℃ (96.8kPa). Soluble in organic solvents such as alcohol and ether, but insoluble in water. Iodine can be easily separated and analyzed by light.

Uses

4-Iodoanisole is used in wide range of medicals industrial applications as well as in human and animal nutrition products, pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals. Iodine derivatives are also used as organic building blocks, analytical reagents.

Preparation

4-Iodoanisole is synthesized by the reaction of anisole with iodine chloride. Add anisole to glacial acetic acid, stir and slowly add iodine chloride. After the addition was completed, the temperature was refluxed for 3.5h. Cool, pour into ice water, and precipitate p-iodoanisole. After it was separated, the free iodine was washed with 5% sodium sulfite, then washed with water, distilled under reduced pressure, and the fractions with a boiling point of 140-160 °C (5.33 kPa) were collected and cooled to 0 °C for filtration. Wash with methanol and recrystallize to obtain the finished product.

Definition

ChEBI: (alpha-D-mannosyl)7-beta-D-mannosyl-diacetylchitobiosyl-L-asparagine, isoform B (protein) is a member of methoxybenzenes.

Synthesis Reference(s)

The Journal of Organic Chemistry, 58, p. 2058, 1993 DOI: 10.1021/jo00060a020
Tetrahedron Letters, 27, p. 3497, 1986 DOI: 10.1016/S0040-4039(00)84832-7

Purification Methods

Crystallise 4-iodoanisole from aqueous EtOH and/or distil it under vacuum. [Beilstein 6 H 208, 6 I 109, 6 II 199, 6 III 744, 6 IV 1075.]

4-Iodoanisole Preparation Products And Raw materials

Raw materials

Sodium sulfite Iodine monochloride Dimethyl ether

Preparation Products

4-Allylanisole Benzeneacetic acid, α-acetyl-4-methoxy-, ethyl ester 4-BROMO-4'-METHOXYBENZOPHENONE Ethyl 4-methoxycinnamate 6-Methoxy-2-(4-methoxyphenyl)benzobithiophene

4,4'-DIMETHOXYDIPHENYLAMINE (4-METHOXYPHENYLETHYNYL)TRIMETHYLSILANE& 4,4'-Dimethoxybiphenyl 1H-Benzimidazole,1-butyl-(9CI) 1-(4-METHOXYPHENYL)-1H-IMIDAZOLE

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4-Iodoanisole Suppliers

Global( 417)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Hebei Mojin Biotechnology Co., Ltd	+8613288715578	sales@hbmojin.com	China	12470	58
Henan Fengda Chemical Co., Ltd	+86-371-86557731 +86-13613820652	info@fdachem.com	China	16799	58
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	15965	58
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21689	55
Hangzhou FandaChem Co.,Ltd.	008657128800458; +8615858145714	fandachem@gmail.com	China	9342	55
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29914	58
Shenzhen Nexconn Pharmatechs Ltd	+86-755-89396905 +86-15013857715	admin@nexconn.com	China	10248	58
Accela ChemBio Inc.	(+1)-858-699-3322	info@accelachem.com	United States	19965	58
Hebei Guanlang Biotechnology Co., Ltd.	+86-19930503282	alice@crovellbio.com	China	8822	58
Chongqing Chemdad Co., Ltd	+86-023-61398051 +8613650506873	sales@chemdad.com	China	39916	58

Supplier	Advantage
Hebei Mojin Biotechnology Co., Ltd	58
Henan Fengda Chemical Co., Ltd	58
Shanghai Daken Advanced Materials Co.,Ltd	58
Henan Tianfu Chemical Co.,Ltd.	55
Hangzhou FandaChem Co.,Ltd.	55
career henan chemical co	58
Shenzhen Nexconn Pharmatechs Ltd	58
Accela ChemBio Inc.	58
Hebei Guanlang Biotechnology Co., Ltd.	58
Chongqing Chemdad Co., Ltd	58

View Lastest Price from 4-Iodoanisole manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2023-12-24	4-Iodoanisole 696-62-8	US $100.00-1.00 / KG	1KG	99%	g-kg-tons, free sample is available	Henan Fengda Chemical Co., Ltd
2023-09-06	4-Iodoanisole 696-62-8	US $0.00 / KG	1KG	99%	50000KG/month	Hebei Mojin Biotechnology Co., Ltd
2021-07-13	4-Iodoanisole 696-62-8	US $15.00-10.00 / KG	1KG	99%+ HPLC	Monthly supply of 1 ton	Zhuozhou Wenxi import and Export Co., Ltd

4-Iodoanisole
696-62-8
US $100.00-1.00 / KG
99%
Henan Fengda Chemical Co., Ltd

4-Iodoanisole
696-62-8
US $0.00 / KG
99%
Hebei Mojin Biotechnology Co., Ltd

4-Iodoanisole
696-62-8
US $15.00-10.00 / KG
99%+ HPLC
Zhuozhou Wenxi import and Export Co., Ltd

4-Iodoanisole Spectrum

4-Iodoanisole(696-62-8)MS 4-Iodoanisole(696-62-8)¹HNMR 4-Iodoanisole(696-62-8)¹³CNMR 4-Iodoanisole(696-62-8)IR1 4-Iodoanisole(696-62-8)IR2 4-Iodoanisole(696-62-8)Raman

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1-iodo-4-methoxy-benzen 4-Iodophenyl methyl ether, 4-Methoxyiodobenzene Methyl(4-iodophenyl) ether 4-Iodoanisole p-Iodoanisole Of iodine anisole 1-Iodo-4-methoxybenzene, 4-Iodophenyl methyl ether 4-iodoaisole 4-Iodoanisole, 98% 100GR 4-Iodoanisole, 98% 25GR 4-iodoether 4-Iodoanisole, 99.5% cAMP-responsive element modulator CREM-α 4-Iodophenyl methyl ether 4-Methoxyiodobenzene 1-Iodo-4-methoxybenzene 4-Iodomethoxybenzene 4-Methoxyphenyl iodide Anisole, 4-iodo- Anisole, p-iodo- anisole,4-iodo- p-Iodomethoxybenzene p-Iodophenyl methyl ether p-Methoxyiodobenzene p-Methoxyphenyl iodide 4-IODOANISOLE 4-IODOPHENYL METHYL ETHER AURORA KA-7366 BENZENE, 1-IODO-4-METHOXY- 4-Iodoanisole,~99% 4-Iodoanisole,98+% 4-IODOANISOLE / 1-IODO-4-METHOXYBENZENE PARA IODO ANISOLE 4-Iodoanisole> 4-lodoanisole P-IODOANISOLE 1-IODO-4-METHOXYBENZENE 4-IODANISOLE 4-IODOANISOL 4-METHOXYIODOBENZENE p-iodoanisol Isoform 4-Idiobenzyl ether Guaiacol Impurity 13 Acetylsalicylic Acid Impurity 16 696-62-8 696-42-8 IC6H4OCH3 ETHER Ethers Organic Building Blocks Oxygen Compounds Building Blocks Pyridines ,Halogenated Heterocycles Building Blocks C2 to C8 Chemical Synthesis Ethers Organic Building Blocks Oxygen Compounds