methyl 6-(bromomethyl)nicotinate
methyl 6-(bromomethyl)nicotinate 物理性質
- 沸点 :
- 284.9±30.0℃ (760 Torr)
- 比重(密度) :
- 1.533±0.06 g/cm3 (20 ºC 760 Torr)
- 闪点 :
- 126.1±24.6℃
- 貯蔵温度 :
- under inert gas (nitrogen or Argon) at 2-8°C
- 酸解離定数(Pka):
- 1.40±0.22(Predicted)
- 外見 :
- solid
- 色:
- OFF WHITE
methyl 6-(bromomethyl)nicotinate 価格
もっと(11)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQE-2775 |
Methyl 6-(bromomethyl)nicotinate |
131803-48-0 |
250mg |
￥30000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQE-2775 |
Methyl 6-(bromomethyl)nicotinate |
131803-48-0 |
5g |
￥235000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01COBQE-2775 |
Methyl 6-(bromomethyl)nicotinate |
131803-48-0 |
10g |
￥405000 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOOR346134 |
Methyl 6-(bromomethyl)nicotinate |
131803-48-0 |
1g |
￥129600 |
2023-06-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01MAS058783 |
6-Bromomethyl-nicotinic acid methyl ester |
131803-48-0 |
1g |
￥148100 |
2024-03-01 |
購入 |
methyl 6-(bromomethyl)nicotinate 化学特性,用途語,生産方法
合成
methyl 6-(bromomethyl)nicotinate is synthesised using methyl 6-methylnicotinate as a raw material by chemical reaction. The specific synthesis steps are as follows:
0.471 g (1.0 equivalent) of N-bromosuccinimide and 64 mg (0.1 equivalent) of benzoyl peroxide are added to a solution of 0.4 g of the product obtained in the preceding Stage 1 in 15 ml of carbon tetrachloride. The solution is brought to reflux for 6 hours, then filtered and evaporated under reduced pressure. The residue is purified by chromatography on silica gel (dichloromethane/ethyl acetate: 95/5) to produce 0.262 g of the expected product. [ Yield: 43percent MS: MH+ 231].
methyl 6-(bromomethyl)nicotinate 上流と下流の製品情報
原材料
準備製品
methyl 6-(bromomethyl)nicotinate 生産企業
Global( 106)Suppliers
131803-48-0()キーワード:
- 131803-48-0
- methyl 6-(bromomethyl)nicotinate
- 6-Bromomethyl-nicotinic acid methyl ester
- 3-Pyridinecarboxylic acid, 6-(broMoMethyl)-
- 6-(bromomethyl)-3-pyridinecarboxylic acid methyl ester
- Methyl 2-(bromomethyl)pyridine-5-carboxylate
- 6-Bromomethylpyridin-3-carboxylic acid methyl ester
- 3-Pyridinecarboxylic acid, 6-(bromomethyl)-, methyl ester