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Postion:Product Catalog >Organic Chemistry>Heterocyclic Compounds>1-Boc-3-piperidone
1-Boc-3-piperidone
  • 1-Boc-3-piperidone
  • 1-Boc-3-piperidone
  • 1-Boc-3-piperidone
  • 1-Boc-3-piperidone
  • 1-Boc-3-piperidone

1-Boc-3-piperidone NEW

Price Get Latest Price
Package 1KG 5KG 25KG
Min. Order: 1KG
Supply Ability: 20 T each week
Update Time: 2023-08-12

Product Details

Product Name: 1-Boc-3-piperidone CAS No.: 98977-36-7
EC-No.: 629-575-1 Min. Order: 1KG
Purity: 98%~99% Supply Ability: 20 T each week
Release date: 2023/08/12

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Product Name:1-Boc-3-piperidone
Synonyms:T-BUTYL-3-PIPERIDONE-1-CARBOXYLATE;TERT-BUTYL 3-OXOPIPERIDINE-1-CARBOXYLATE;N-Boc-3-piperidone;N-BOC-3-PIPERIDINONE;3-OXOPIPERIDINE, N-BOC PROTECTED;3-OXO-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER;1-PIPERIDINECARBOXYLIC ACID, 3-OXO-, 1,1-DIMETHYLETHYL ESTER;1-N-BOC-3-PIPERIDONE
CAS:98977-36-7
MF:C10H17NO3
MW:199.25
EINECS:629-575-1
Product Categories:Pyrans, Piperidines & Piperazines;Building Blocks;Piperidine;Piperidines;Heterocyclic Building Blocks;Piperidones;Acids and Derivatives;Carbonyl Compounds;pharmacetical;Pyrans, Piperidines &Piperazines;Pharmaceutical Intermediates;98977-36-7
Mol File:98977-36-7.mol
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1-Boc-3-piperidone Chemical Properties
Melting point 35-40 °C (lit.)
Boiling point 289.8±33.0 °C(Predicted)
density 1.099±0.06 g/cm3(Predicted)
Fp >230 °F
storage temp. 2-8°C
pka-1.71±0.20(Predicted)
form Liquid
color Clear colorless
Water Solubility It is insoluble in water.
BRN 5936353
InChIInChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3
InChIKeyRIFXIGDBUBXKEI-UHFFFAOYSA-N
SMILESN1(C(OC(C)(C)C)=O)CCCC(=O)C1
CAS DataBase Reference98977-36-7(CAS DataBase Reference)

Safety Information
Safety Statements 24/25
WGK Germany 3
HazardClass KEEP COLD
HS Code 29339900


1-Boc-3-piperidone Usage And Synthesis
Chemical PropertiesWhite to yellow low melting solid
Uses1-Boc-3-piperidone, is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff.
SynthesisWith 179g compound 3(1-BOC-3-piperidines alcohol) drop in the 2L reaction flask, drop into pimelinketone 1300g, aluminum isopropylate 88g, methylene dichloride 400ml is warming up to 80 ℃, insulation reaction 8h, reaction finishes to be cooled to room temperature, adds 10% sodium hydroxide 200ml, stirring at normal temperature 30min, filter, the filtrate normal pressure reclaims methylene dichloride, reclaim under reduced pressure pimelinketone again, reclaim finish after, add the 300ml dichloromethane extraction three times, it is dry concentrated to merge oil reservoir, gets 1-BOC-3-piperidone crude product.
Refining: with 1-BOC-3-piperidone crude product is that 60pa, temperature are to distill under 104 ~ 105 ℃ the condition at pressure, gets 1-BOC-3-piperidone elaboration 163g, 92.9%.

1-Boc-3-piperidone Preparation Products And Raw materials
Preparation Products(S)-3-Amino-1-N-Boc-piperidine-->3-HYDROXY-3-PHENYL-PIPERIDINE-->6-METHOXY-1,2,3,4-TETRAHYDRO-BETA-CARBOLINE-->4,5,6,7-tetrahydro-1-methyl-1H-Pyrazolo[3,4-c]pyridine-->Acetone-->tert-butyl 3-(isopropylamino)piperidine-1-carboxylate-->5-(Toluene-4-sulfonyloxy)-3,4-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester-->TERT-BUTYL 3-(N-BENZYL-N-METHYLAMINO) PIPERIDINE-1-CARBOXYLATE-->1-N-BOC-3-HYDROXY-3-PHENYLPIPERIDINE





Company Profile Introduction

Shandong Huisheng Import & Export Co., Ltd. is located in Jinan city, Shandong Province, is a collection of domestic trade, international trade in one of the diversified services company. Our goal is to provide customers with high quality solutions and one-stop purchasing experience. At present, the company business scope involves five areas: Organic chemical raw materials, inorganic chemical raw materials, fine chemical raw materials, dangerous chemicals and green environmental protection chemical technology project promotion, and we has also established good relations of cooperation with several well-known enterprises and won the strong support of extensive trust from the new and old customers. Products are widely used in automobile, household appliances, office supplies, mobile phone accessories, routers, food, medical and other fields. At present, our business covers 30 countries, and our customers mainly come from Australia, New Zealand, Canada, Germany, France, Poland, South Korea, Russia, Bangladesh, Vietnam, Kazakhstan, India, Ghana, Nigeria, South Africa, Egypt and other more than 30 countries. The company has a sound quality management system and advanced professional equipment, with a positive attitude to meet the changing needs of customers. We take "quality products, quality service, competitive price, timely delivery" as the purpose, looking forward to greater cooperation with overseas customers on the basis of mutual benefit. Our company provides a wide range of products to meet your various needs. Since its inception, the company has always adhered to the "quality first, customer first, reputation first" business policy, wholeheartedly meet the potential needs of our customers. Under the irresistible situation of economic globalization, our company is willing to cooperate sincerely with enterprises around the world to achieve a win-win situation.

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