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ChemicalBook CAS DataBase List 1-(2,4-DICHLORO-PHENYL)-ETHYLAMINE

1-(2,4-DICHLORO-PHENYL)-ETHYLAMINE synthesis

1synthesis methods
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Yield:-

Steps:

22 EXAMPLE 22
Content of the oil 1-(2',4'-dichlorophenyl)ethylamine; 91%, 1-(4'-chlorophenyl)ethylamine 2.9%, N-1-(2',4'-dichlorophenyl)ethyl-α-(2',4'-dichlorophenyl)ethylamine; 1.1%, N-acetyl-α-(2',4'-dichlorophenyl)ethylamide; 1.5%, an alcohol obtained by reduction of carbonyl group; not detected. 58.5 g of 1-(2',4'-dichlorophenyl)ethylamine was obtained by distillation; the purity: 99%, boiling point: 130°-132° C./20 mmHg.

References:

Sumitomo Chemical Company, Limited US5739401, 1998, A

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