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ChemicalBook CAS DataBase List 1-Benzyl-5-ethoxyhydantoin

1-Benzyl-5-ethoxyhydantoin synthesis

2synthesis methods
-

Yield:-

Reaction Conditions:

Stage #1:benzylurea;Glyoxilic acid;2,2-dihydroxyacetic acid with acetic acid in water at 100; for 2 h;
Stage #2:orthoformic acid triethyl ester with sulfuric acid in ethanol at 80; for 1 h;
Stage #3: in hexane;ethyl acetate at 3 - 25; for 11 h;

References:

Bayer Aktiengesellschaft US6365752, 2002, B1 Location in patent:Example 3

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