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ChemicalBook CAS DataBase List 1-BUTEN-3-YNE

1-BUTEN-3-YNE synthesis

12synthesis methods
Acetylene is dimerized in the presence of hydrochloric acid solution of cuprous chloride and ammonium chloride to obtain vinylacetylene.
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Yield:689-97-4 70%

Reaction Conditions:

with potassium hydroxide;2,3-dimethyl-2,3-butane diol;Aliquat 336 in Petroleum ether; for 1.5 h;Heating;

References:

Verkruijsse, H.D.;Brandsma, L. [Synthetic Communications,1990,vol. 20,# 21,p. 3355 - 3358]

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