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1-Butylaziridine synthesis

2synthesis methods
-

Yield:1120-85-0 30%

Reaction Conditions:

with chlorosulfonic acid

Steps:

6 6.

6. Preparation of N-(n-butyl)-aziridine (XIX) Compound XIX was prepared from N-(n-butyl)-ethanolamine and chlorosulphonic acid in 30% yield, bpt 29°-30° C./95 mbar, in accordance with the method of Elderfield et al (J Org Chem (1949), 605-637). 1 H nmr and ir spectra were in agreement with the assigned structure.

References:

US4985584,1991,A