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ChemicalBook CAS DataBase List 1-Eth-1-ynyl-4-(pentyloxy)benzene

1-Eth-1-ynyl-4-(pentyloxy)benzene synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: KOH / ethanol; H2O
2: triphenylphosphine; triethylamine / bis(triphenylphosphine) palladium dichloride; copper(I) iodide / tetrahydrofuran / 2 h / Heating
3: KOH / toluene / Heating

References:

Yang;Tang;Gong;Wen [Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals,2000,vol. 348,p. 153 - 165]

116223-55-3 Synthesis
Benzene, 1-iodo-4-(pentyloxy)-

116223-55-3
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