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ChemicalBook CAS DataBase List 1-Methylcaffeine

1-Methylcaffeine synthesis

10synthesis methods
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Yield: 52%

Reaction Conditions:

with (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate;trifluoroacetic acid in acetonitrile at 30;Inert atmosphere;Irradiation;

References:

DiRocco, Daniel A.;Dykstra, Kevin;Krska, Shane;Vachal, Petr;Conway, Donald V.;Tudge, Matthew [Angewandte Chemie - International Edition,2014,vol. 53,# 19,p. 4802 - 4806] Location in patent:supporting information

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