ChemicalBook CAS DataBase List (R )-(2-Amino-1-phenyl-ethyl)-carbamic acid benzyl ester

(R )-(2-Amino-1-phenyl-ethyl)-carbamic acid benzyl ester synthesis

5synthesis methods

Product Name:(R )-(2-Amino-1-phenyl-ethyl)-carbamic acid benzyl ester
CAS Number:130406-35-8
Molecular formula:C16H18N2O2
Molecular Weight:270.33

56613-80-0
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(R )-(2-Amino-1-phenyl-ethyl)-carbamic acid benzyl ester

130406-35-8
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 87 percent / Et₃N / tetrahydrofuran / 18 h / Ambient temperature
2: Et₃N / CH₂Cl₂ / 18 h / Ambient temperature
3: NaN₃ / dimethylformamide / 3 h / 80 °C
4: Lindlar catalyst, H₂ / ethyl acetate / 6 h / 30 °C / 2327.2 Torr

References:

Horwell, David C.;Hughes, John;Hunter, John C.;Pritchard, Martyn C.;Richardson, Reginald S.;at al. [Journal of Medicinal Chemistry,1991,vol. 34,# 1,p. 404 - 414]

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References

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References