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[2-(1-methyl-1H-benzimidazol-2-yl)ethyl]amine dihydrochloride synthesis

1synthesis methods
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Yield:138078-14-5 97%

Reaction Conditions:

Stage #1: N-methyl-1,2-phenylenediamine;3-amino propanoic acidwith hydrogenchloride in water; for 96 h;Reflux;
Stage #2: in ethanol;water at 8; for 24 h;

References:

Schottenheim, Julia;Fateeva, Natalie;Thimm, Wulf;Krahmer, Jan;Tuczek, Felix [Zeitschrift fur Anorganische und Allgemeine Chemie,2013,vol. 639,# 8-9,p. 1491 - 1497]