ChemicalBook CAS DataBase List (E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide

(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide synthesis

5synthesis methods

Product Name:(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide
CAS Number:1417997-93-3
Molecular formula:C22H19NO3
Molecular Weight:345.39

531-59-9 Synthesis

531-59-9
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(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide

1417997-93-3
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$35.00/1mg

Yield:-

Steps:

Multi-step reaction with 6 steps
1: 6 h / Inert atmosphere
2: pyridine / dichloromethane / 2 h / 20 °C
3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C
4: lithium hydroxide / methanol
5: triethylamine / tetrahydrofuran / 1 h / 20 °C
6: hydroxylamine hydrochloride; potassium hydroxide / methanol / 3 h / 20 °C

References:

Huang, Wei-Jan;Wang, Yi-Ching;Chao, Shi-Wei;Yang, Chen-Yui;Chen, Liang-Chieh;Lin, Mei-Hsiang;Hou, Wen-Chi;Chen, Mei-Yu;Lee, Tai-Lin;Yang, Ping;Chang, Chung-I [ChemMedChem,2012,vol. 7,# 10,p. 1815 - 1824]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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1417997-93-3
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References

1000210-73-0
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1417997-93-3
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References

2-Propenoic acid, 3-(2-hydroxy-4-methoxyphenyl)-, ethyl ester, (E)-

139386-27-9
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1417997-93-3
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References

1000210-73-0
0 suppliers
inquiry

1417997-93-3
62 suppliers
$35.00/1mg

References