1H-INDOLE-3-CARBOXYLIC ACID, 6-METHYL-1-(PHENYLMETHYL)-,METHYL ESTER synthesis

2synthesis methods

Product Name:1H-INDOLE-3-CARBOXYLIC ACID, 6-METHYL-1-(PHENYLMETHYL)-,METHYL ESTER
CAS Number:163083-64-5
Molecular formula:C18H17NO2
Molecular Weight:279.33

942-24-5
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1H-INDOLE-3-CARBOXYLIC ACID, 6-METHYL-1-(PHENYLMETHYL)-,METHYL ESTER

163083-64-5
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 96 percent / K₂CO₃ / dimethylformamide
2: 31 percent / Br₂ / 2 h / 0 °C
3: 91 percent / AlCl₃ / CH₂Cl₂ / 0.5 h / -20 °C
4: 76 percent / Raney Ni / methanol / 0.17 h / 25 °C

References:

Hirano, Satoshi;Akai, Ritsuko;Shinoda, Yoshihiko;Nakatsuka, Shin-ichi [Heterocycles,1995,vol. 41,# 2,p. 255 - 258]

1H-Indole-3-carboxylic acid, 1-(phenylmethyl)-, methyl ester

155134-26-2
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163083-64-5
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References