Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2-(2-chlorophenyl)cyclohexanone

2-(2-chlorophenyl)cyclohexanone synthesis

5synthesis methods
To a flame dried flask was added Cs2CO3 (6.5 g, 20 mmol), Pd2(dba)3 (184 mg, 0.2 mmol) and Xantphos (139 mmol, 0.24 mmol). After purging with N2, toluene (10 mL), ketone (15 mmol) and phenyl iodide (1.11 mL, 10 mmol) were added. After stirring overnight at 80 .MALE.C, the mixture was filtered and concentrated in vacuo to afford a residue, which was purified by flash chromatography to provide the desired 2-(2-chlorophenyl)cyclohexanone.
synthesis of 2-(2-chlorophenyl)cyclohexanone
694-80-4 Synthesis
2-Bromochlorobenzene

694-80-4
391 suppliers
$5.00/10g

2-(2-chlorophenyl)cyclohexanone

91393-49-6
92 suppliers
inquiry

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: tert.-butyl lithium / tetrahydrofuran / 5 h / -90 °C
1.2: 0 °C
2.1: Dess-Martin periodane / dichloromethane

References:

Lanzhou University;Zhang Fumin;Peng Rui;Zhang Zhiqiang CN106478367, 2017, A

694-80-4 Synthesis
2-Bromochlorobenzene

694-80-4
391 suppliers
$5.00/10g

108-94-1 Synthesis
Cyclohexanone

108-94-1
526 suppliers
$12.00/50g

2-(2-chlorophenyl)cyclohexanone

91393-49-6
92 suppliers
inquiry

References
22568-07-6 Synthesis
1-chloro-2-[(E)-2-nitroethenyl]benzene

22568-07-6
27 suppliers
inquiry

2-(2-chlorophenyl)cyclohexanone

91393-49-6
92 suppliers
inquiry

References
286-20-4 Synthesis
Cyclohexene oxide

286-20-4
198 suppliers
$14.00/25mL

2-(2-chlorophenyl)cyclohexanone

91393-49-6
92 suppliers
inquiry

References
Benzene, 1-chloro-2-(2-nitrocyclohexyl)-

91494-54-1
0 suppliers
inquiry

2-(2-chlorophenyl)cyclohexanone

91393-49-6
92 suppliers
inquiry

References