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ChemicalBook CAS DataBase List 2-[2-(DIPHENYLPHOSPHINO)ETHYL]PYRIDINE

2-[2-(DIPHENYLPHOSPHINO)ETHYL]PYRIDINE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: potassium carbonate; Methyltriphenylphosphonium bromide / 1,4-dioxane / 16 h / Reflux
2: (μ-oxo)bis[(1,2-ethanediamino-N,N'-bis(salicylidene))iron(III)] / acetonitrile / 72 h / 20 °C / Inert atmosphere; Glovebox; Schlenk technique

References:

Gallagher;Webster [Chemical Communications,2014,vol. 50,# 81,p. 12109 - 12111]