2,4-dihydroxy-6-n-butylbenzoic acid, methyl ester synthesis
2synthesis methods
- Product Name:2,4-dihydroxy-6-n-butylbenzoic acid, methyl ester
- CAS Number:102342-62-1
- Molecular formula:C12H16O4
- Molecular Weight:224.25
![3,9-Dioxa-2,10-disilaundeca-4,6-diene, 4-methoxy-2,2,10,10-tetramethyl-8-methylene-6-[(trimethylsilyl)oxy]-](/CAS/20210111/GIF/102342-54-1.gif)
Yield:102342-62-1 38%
Reaction Conditions:
with titanium tetrachloride in dichloromethane;1.) -78 deg C, 2-3 h, 2.) RT, overnight;
References:
Chan, T. H.;Stoessel, D. [Journal of Organic Chemistry,1986,vol. 51,# 13,p. 2423 - 2428]
