2-DI-TERT-BUTYLPHOSPHINO-3,4,5,6-TETRAM& synthesis
- Product Name:2-DI-TERT-BUTYLPHOSPHINO-3,4,5,6-TETRAM&
- CAS Number:857356-94-6
- Molecular formula:C33H53P
- Molecular Weight:480.75
488-23-3
145 suppliers
$13.00/1g
857356-94-6
141 suppliers
$20.00/100mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 85 percent / bromine; ZnCl2 / acetic acid / 14 h / 20 °C
2.1: magnesium; 1,2-dibromoethane / tetrahydrofuran / 1.5 h / 60 °C
2.2: tetrahydrofuran / 1.5 h / 60 °C
2.3: 62 percent / CuCl / tetrahydrofuran / 40 h / 75 °C
References:
Burgos, Carlos H.;Barder, Timothy E.;Huang, Xiaohua;Buchwald, Stephen L. [Angewandte Chemie - International Edition,2006,vol. 45,# 26,p. 4321 - 4326]
13716-10-4
257 suppliers
$22.00/1 g
21524-34-5
264 suppliers
$6.00/5g
36321-73-0
51 suppliers
$61.00/500mg
857356-94-6
141 suppliers
$20.00/100mg