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(2E,8E)-2,8-Decadiene-4,6-diyn-1-ol acetate synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 84.4 percent / 1N KOH / methanol / 5 h / Ambient temperature
2: 1.) n-BuNH2, NH2OH*HCl, CuCl / 1.) MeOH; 2.) 1 h
3: 95 percent

References:

Carpita, Adriano;Neri, Dario;Rossi, Renzo [Gazzetta Chimica Italiana,1987,vol. 117,# 8,p. 481 - 490]