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ChemicalBook CAS DataBase List 3,3'-Dihydroxybenzidine

3,3'-Dihydroxybenzidine synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: sulfuric acid; sodium nitrite; copper(II) sulfate / isopropyl alcohol; ethyl acetate / Heating; Large scale
2.1: sulfuric acid; sodium iodide; dihydrogen peroxide / methanol / 34 - 38 °C / Large scale
3.1: palladium on activated charcoal; triethylamine / toluene / Heating; Large scale
4.1: ammonium hydroxide / 100 - 110 °C / 750.08 - 2250.23 Torr / Large scale
4.2: 20 - 70 °C / pH 3-4 / Large scale

References:

CN110156712,2019,A

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