3,5-DIACETOXYBENZOIC ACID synthesis
- Product Name:3,5-DIACETOXYBENZOIC ACID
- CAS Number:35354-29-1
- Molecular formula:C11H10O6
- Molecular Weight:238.19
Yield: 92%
Reaction Conditions:
with triethylamine at 90 - 100; for 0.166667 h;Reagent/catalyst;
Steps:
1.1 Preparation of 3,5-diacetoxybenzoic acid
A mixture of 7.7 g (0.05 mol) of 3,5-dihydroxybenzoic acid (1), 25 mL of acetic anhydride and 2 mL of triethylamine was mixed and stirred for 10 min and heated at 90 to 100 ° C. TLC was monitored. Product into the ice water, a large number of white precipitate generated, filtered to obtain a white solid is the crude product,Recrystallization from ethanol gave 11.0 g of white crystals (2) in 92% yield.
References:
Tianjin Polytechnic University;QI, DONGLAI;WANG, XIANG CN105884580, 2016, A Location in patent:Paragraph 0007; 0011; 0012
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
99-10-5
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$5.00/5g
35354-29-1
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$22.00/1g
