(3-Bromo-2-nitrophenyl)methanol synthesis
- Product Name:(3-Bromo-2-nitrophenyl)methanol
- CAS Number:1261475-45-9
- Molecular formula:C7H6BrNO3
- Molecular Weight:232.03
Yield:1241894-37-0 610 mg
Reaction Conditions:
Stage #1: m-bromobenzoic acidwith sulfuric acid;nitric acid at 0;
Stage #2: with borane-THF in tetrahydrofuran at 20;Inert atmosphere;
Stage #3: with methanol in tetrahydrofuran;
References:
Jacquart, Aurelie;Tauc, Patrick;Pansu, Robert B.;Ishow, Elena [Chemical Communications,2010,vol. 46,# 24,p. 4360 - 4362] Location in patent:supporting information; experimental part
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