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ChemicalBook CAS DataBase List 3-Pyridinemethanamine,6-methoxy-(9CI)

3-Pyridinemethanamine,6-methoxy-(9CI) synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium carbonate / 1,4-dioxane; water / 36 h / Reflux
2: ethylenediamine / 1,4-dioxane; propan-1-ol; water / 24 h / Reflux

References:

Murai, Norio;Miyano, Masayuki;Yonaga, Masahiro;Tanaka, Keigo [Organic Letters,2012,vol. 14,# 11,p. 2818 - 2821]