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[2-(bromomethyl)-2-(2,4-dichlorophenyl)-1,3-dioxolan-4-yl]methyl benzoate synthesis

3synthesis methods
Ketoconazole Impurity 7

172032-21-2
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[2-(bromomethyl)-2-(2,4-dichlorophenyl)-1,3-dioxolan-4-yl]methyl benzoate

331949-30-5
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: Br2 / benzene / 0.5 h
2: 2 h / Ambient temperature

References:

Chapman, David R.;Bauer, Ludwig [Journal of Heterocyclic Chemistry,1990,vol. 27,# 7,p. 2053 - 2061]