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4-(2-OXO-PROPYL)-BENZOIC ACID ETHYL ESTER synthesis

6synthesis methods
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Yield: 71%

Reaction Conditions:

Stage #1:p-aminoethylbenzoate with methanesulfonic acid;2,2-dimethylpropyl nitrite in water;acetone at 25; for 0.166667 h;Green chemistry;
Stage #2:Isopropenyl acetate in water;acetone at 20; for 6 h;Irradiation;Green chemistry;

References:

Wang, Liang;Shen, Jun;Yang, Sen;Liu, Wenjie;Chen, Qun;He, Mingyang [Green Chemistry,2018,vol. 20,# 6,p. 1290 - 1296] Location in patent:supporting information