ChemicalBook CAS DataBase List 1-[9-Ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]ethanone 1-(O-acetyloxime)

1-[9-Ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]ethanone 1-(O-acetyloxime) synthesis

4synthesis methods

Product Name:1-[9-Ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]ethanone 1-(O-acetyloxime)
CAS Number:478556-66-0
Molecular formula:C26H24N2O3
Molecular Weight:412.48

1-[9-Ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]ethanone 1-(O-acetyloxime) can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly in laboratory research and chemical industry during production process. It can be synthesized from N-Ethylcarbazole and chlorobenzene catalyzed by zirconium catalyst.

86-28-2 Synthesis

86-28-2
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1-[9-Ethyl-6-(2-methylbenzoyl)-9H-carbazol-3-yl]ethanone 1-(O-acetyloxime)

478556-66-0
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: zirconium catalyst / chlorobenzene / 1 h / 15 - 20 °C
2: chlorobenzene / 0.5 h
3: hydroxylamine hydrochloride; potassium dihydrogenphosphate / water; propan-1-ol / Reflux
4: boric acid / chlorobenzene; water / Reflux

References:

CN105566201,2016,A