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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

5-[4-(Dimethylamino)phenyl]-2-pyridinamine synthesis

1synthesis methods
1072-97-5 Synthesis
2-Amino-5-bromopyridine

1072-97-5
697 suppliers
$9.00/1g

4-(Dimethylamino)phenylboronic acid

28611-39-4
215 suppliers
$38.43/1G

5-[4-(Dimethylamino)phenyl]-2-pyridinamine

503536-77-4
20 suppliers
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Yield:503536-77-4 54%

Reaction Conditions:

with bis-triphenylphosphine-palladium(II) chloride;sodium carbonate in 1,4-dioxane;water at 90; for 10 h;Inert atmosphere;

References:

Chen, Xing;Yan, Yaoyao;Zhang, Zhaoyan;Zhang, Faming;Liu, Mingming;Du, Leran;Zhang, Haixia;Shen, Xiaobao;Zhao, Dahai;Shi, Jing Bo;Liu, Xinhua [Journal of Medicinal Chemistry,2021,vol. 64,# 16,p. 11857 - 11885]