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ChemicalBook CAS DataBase List Methyl 4-chloro-3-methoxy-5-nitrobenzenecarboxylate

Methyl 4-chloro-3-methoxy-5-nitrobenzenecarboxylate synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 74 percent / HNO3, glacial acetic acid / acetic acid / 2 h / Ambient temperature
2: 88 percent / oxalyl chloride / dimethylformamide / -20 deg C; 80 deg C, 3 h

References:

Meyers;Babiak;Campbell;et al. [Journal of the American Chemical Society,1983,vol. 105,# 15,p. 5015 - 5024]