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CARBAMIC ACID, N-(4,6-DIMETHYL-2-PYRIDINYL)-,1,1-DIMETHYLETHYL ESTER synthesis

2synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
816 suppliers
$13.50/25G

5407-87-4 Synthesis
2-Amino-4,6-dimethylpyridine

5407-87-4
200 suppliers
$9.00/1g

CARBAMIC ACID, N-(4,6-DIMETHYL-2-PYRIDINYL)-,1,1-DIMETHYLETHYL ESTER

848472-36-6
7 suppliers
$57.70/1g

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Yield:848472-36-6 85%

Reaction Conditions:

in tert-butyl alcohol;

Steps:

4.A

Figure 4 illustrates various schemes (A, B, and C) for synthesizing exemplary compounds (A) 4 and (B) 5 of the present invention.

References:

WO2008/36294,2008,A2 Location in patent:Page/Page column 4; 5/8