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ChemicalBook CAS DataBase List (-)-Benzotetramisole

(-)-Benzotetramisole synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine / 48 h / 135 °C / Inert atmosphere
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere
2.2: 0.5 h / 20 °C / Inert atmosphere
2.3: 12 h / 55 °C / Inert atmosphere

References:

Matsumoto, Takuya;Urano, Yasuteru;Takahashi, Yoshinori;Mori, Yusuke;Terai, Takuya;Nagano, Tetsuo [Journal of Organic Chemistry,2011,vol. 76,# 10,p. 3616 - 3625]

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