Bromoniumyl synthesis

6synthesis methods

Product Name:Bromoniumyl
CAS Number:12258-64-9
Molecular formula:BrH
Molecular Weight:80.91

831-23-2 Synthesis

831-23-2
13 suppliers
$641.78/10MG

12258-64-9
0 suppliers
inquiry

Yield:12258-64-9 5715 g

Reaction Conditions:

in water at 124;Temperature;Solvent;

Steps:

7-8 The concentrated recovery of bromination reaction solution:

The reaction solution after the bromination reaction of Example 2, Example 4, and Example 6 was added to a 10-liter four-neck distillation flask, and heated and distilled under stirring,After steaming 0.6 liter of pre-distillate water at 124 ° C, the cold water bath was lowered to normal temperature to obtain 5715 grams of pale yellow hydrobromic acid.Analysis of hydrogen bromide content of 43.2%; free bromine 240ppm.

References:

CN113683491,2021,A Location in patent:Paragraph 0072-0073

7789-31-3 Synthesis