Cyclobutanecarboxylic acid synthesis
- Product Name:Cyclobutanecarboxylic acid
- CAS Number:3721-95-7
- Molecular formula:C5H8O2
- Molecular Weight:100.12
74-85-1
93 suppliers
$79.00/11l
79-10-7
685 suppliers
$20.16/100 mL
3721-95-7
414 suppliers
$7.00/5g
Yield:3721-95-7 97%
Reaction Conditions:
in dichloromethane at -30 - -20; for 3 h;UV-irradiation;Temperature;
Steps:
1 Example 3
72 g acrylic acid into four 500ml glass bottle, 500 g of methylene chloride, topical acetone - dry ice bath cooled to -70 ~ -50 After slowly ethylene gas, was passed rate 137ml / min 4 common hours into 41 g, with violet 450Wfor outer light catalytic high pressure mercury lamp in the control sample GC after the reaction was complete disappearance of starting material acrylic acid to obtain a reaction solution, stopping the flow of ethylenealkenyl gas, turn off the UV lamp, the reaction mixture was distilled atmospheric whole the solvent was removed to give 99.8 g red-brown liquid, by GC analysis, cyclobutylacid purity 98.6%; red-brown liquid was distilled under reduced pressure, vacuum distillation pressure is -0.07 MPa, a temperature of 90 deg.] C; to givea colorless to pale The yellow finished product was 97.1 g of a cyclobutyl formic acid liquid with a GC purity of 99.5% and a yield of 97%
References:
Changzhou Woteng Chemical Technology Co., Ltd.;Wei Xinghong;Sun Fuqiang;Li Honggong;Wang Mingfeng CN107805197, 2018, A Location in patent:Paragraph 0009; 0010-0012
4415-82-1
296 suppliers
$6.00/1g
3721-95-7
414 suppliers
$7.00/5g
120-92-3
401 suppliers
$11.00/25g
3721-95-7
414 suppliers
$7.00/5g
124-38-9
122 suppliers
$175.00/23402
4399-47-7
225 suppliers
$14.14/1gm:
584-08-7
1174 suppliers
$5.00/100g
3721-95-7
414 suppliers
$7.00/5g
2987-17-9
137 suppliers
$10.00/250mg
3721-95-7
414 suppliers
$7.00/5g