Fast Yellow G synthesis
- Product Name:Fast Yellow G
- CAS Number:2512-29-0
- Molecular formula:C17H16N4O4
- Molecular Weight:340.33
102-01-2
8 suppliers
$5.00/100g
89-62-3
221 suppliers
$13.00/25g
2512-29-0
199 suppliers
$103.00/25g
Yield:2512-29-0 99%
Reaction Conditions:
with hydrogenchloride;sodium nitrite in water at 20; for 0.333333 h;Time;
Steps:
1 A method for synthesizing C.I. Pigment Yellow 1 by one-pot method promoted by solid particles, the steps are as follows:
10 g of polytetrafluoroethylene particles (about 70 mg/particle), 1.000 g (1 molar equivalent) of acetoacetanilide, 1.427 g (2.5 molar equivalent) of hydrochloric acid (36%), and 0.944 g (1.1 molar equivalent) were added to the reaction vessel.2-nitro-4-methylaniline, 0.448 g (1.15 molar equivalents) of sodium nitrite,10 mL of water was stirred at room temperature for 20 minutes with a modified mechanical stirring paddle (for improvement of mechanical stirring paddle: ACS Sustainable Chem. Eng. 2016, 4,6754-6762).The reaction was completed by thin-plate chromatography, filtered and rinsed with 3 mL of water, and the filter cake was dried to obtain 1.910 g of C.I.Pigment Yellow 1.The reaction mother liquor and rinse solution are reserved for the next cycle.The product yield is greater than 99%.
References:
Tianjin University;Li Chunbao;Feng Guangyuan CN108912723, 2018, A Location in patent:Paragraph 0037; 0038; 0039; 0051
83-83-0
12 suppliers
$144.00/250mg
102-01-2
8 suppliers
$5.00/100g
89-62-3
221 suppliers
$13.00/25g
2512-29-0
199 suppliers
$103.00/25g