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ChemicalBook CAS DataBase List Licoflavone C

Licoflavone C synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 78 percent / N,N-diisopropylethylamine / dimethylformamide / 1 h / 20 °C
2: 70 percent / tetrabutylammonium hydroxide hydrate / CH2Cl2; toluene / 3 h / 20 °C
3: 56.5 percent / N,N-diethylaniline / 3 h / 217 °C
4: 48 percent / aq. HCl / methanol / 1.5 h / Heating

References:

Daskiewicz, Jean-Baptiste;Depeint, Flore;Viornery, Lionel;Bayet, Christine;Comte-Sarrazin, Geraldine;Comte, Gilles;Gee, Jennifer M.;Johnson, Ian T.;Ndjoko, Karine;Hostettmann, Kurt;Barron, Denis [Journal of Medicinal Chemistry,2005,vol. 48,# 8,p. 2790 - 2804]

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