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ChemicalBook CAS DataBase List Methyl propiolate

Methyl propiolate synthesis

1synthesis methods
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Yield:922-67-8 73%

Reaction Conditions:

Stage #1: propynoic acid methyl esterwith n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2: carbon dioxide in tetrahydrofuran;hexane at 20; for 1 h;

References:

Gherbovet;Sánchez-Murcia, Pedro A.;García Alvarez;Bignon;Thoret;Gago;Roussi [Organic and Biomolecular Chemistry,2015,vol. 13,# 10,p. 3144 - 3154]

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