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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Trimethyl(phenoxy)silane

Trimethyl(phenoxy)silane synthesis

13synthesis methods
General procedure for trimethylsilylation of alcohols with HMDS catalyzed by P2O5/Al2O3. P2O5/Al2O3 (0.1 g) was added to a stirred solution of the alcohol (10 mmol) and HMDS (7.5 mmol) and the mixture was stirred at room temperature for the time specified in Table 2. The reaction was followed by TLC (n-hexane-EtOAc, 9:1). After completion of the reaction, ethyl acetate was added to the reaction mixture and the catalyst was isolated by filtration. It was washed well with ethyl acetate (2 9 5 ml) and then dried at 100°C for 2 h before being used again. The filtered solution was evaporated and purified by passage through a short column of silica gel with n-hexane as eluent (2 x 20 ml). Evaporation of the solvent under reduced pressure gave the pure product Trimethyl(phenoxy)silane, Yield; 89%.
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Azidotrimethylsilane

4648-54-8
293 suppliers
$16.80/5G

108-95-2 Synthesis
Phenol

108-95-2
717 suppliers
$14.00/25g

Trimethyl(phenoxy)silane

1529-17-5
157 suppliers
$9.00/1g

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Yield: 99%

Reaction Conditions:

tetrabutylammomium bromide at 30; for 2.5 h;

References:

Amantini;Fringuelli;Pizzo;Vaccaro [Journal of Organic Chemistry,2001,vol. 66,# 20,p. 6734 - 6737]

999-97-3 Synthesis
Hexamethyldisilazane

999-97-3
631 suppliers
$9.00/5 g

108-95-2 Synthesis
Phenol

108-95-2
717 suppliers
$14.00/25g

Trimethyl(phenoxy)silane

1529-17-5
157 suppliers
$9.00/1g

References
Chlorotrimethylsilane

75-77-4
563 suppliers
$5.04/10

108-95-2 Synthesis
Phenol

108-95-2
717 suppliers
$14.00/25g

Trimethyl(phenoxy)silane

1529-17-5
157 suppliers
$9.00/1g

References
762-72-1 Synthesis
Allyltrimethylsilane

762-72-1
325 suppliers
$10.00/1g

108-95-2 Synthesis
Phenol

108-95-2
717 suppliers
$14.00/25g

Trimethyl(phenoxy)silane

1529-17-5
157 suppliers
$9.00/1g

References
Hexamethyldisilane

1450-14-2
283 suppliers
$29.12/10ML

108-95-2 Synthesis
Phenol

108-95-2
717 suppliers
$14.00/25g

Trimethyl(phenoxy)silane

1529-17-5
157 suppliers
$9.00/1g

References

Trimethyl(phenoxy)silane Related Search:

3-(TERT-BUTYLDIMETHYLSILOXY)THIOPHENOL 1-BROMO-3-(TERT-BUTYLDIMETHYLSILOXY)BENZENE (2-CHLOROPHENOXY)TRIMETHYLSILANE 97 BIS(TRIMETHYLSILYL)BISPHENOL A (4-BROMOPHENOXY)-TERT-BUTYLDIMETHYLSILANE CHLOROMETHYL(2-CHLOROPHENOXY)DIMETHYLSILANE o-(Trimethylsilyl)phenol 2,6-DI([1-(TERT-BUTYL)-1,1-DIPHENYLSILYL]OXY)-9,10-DIHYDROANTHRACENE-9,10-DIONE