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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

Spiro[bicyclo[2.2.1]hept-2-ene-7,2-[1,3]dioxolane] synthesis

2synthesis methods
107-21-1 Synthesis
Ethylene glycol

107-21-1
1302 suppliers
$10.00/25g

Bicyclo[2,2,1]hepten-7-one

694-71-3
8 suppliers
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Spiro[bicyclo[2.2.1]hept-2-ene-7,2-[1,3]dioxolane]

1491-12-9
3 suppliers
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Yield:1491-12-9 89%

Reaction Conditions:

with toluene-4-sulfonic acid in benzene; for 4 h;Heating;

References:

Fujita, Toshiaki;Tanaka, Masakazu;Norimine, Yoshihiko;Suemune, Hiroshi;Sakai, Kiyoshi [Journal of Organic Chemistry,1997,vol. 62,# 12,p. 3824 - 3830]

Bicyclo[2.2.1]hept-2-en-7-ol

53783-87-2
2 suppliers
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Spiro[bicyclo[2.2.1]hept-2-ene-7,2-[1,3]dioxolane]

1491-12-9
3 suppliers
inquiry

References