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ChemicalBook CAS DataBase List TRANS-1,4-CYCLOHEXANEDIMETHANOL

TRANS-1,4-CYCLOHEXANEDIMETHANOL synthesis

8synthesis methods
-

Yield:3236-48-4 72.6%

Reaction Conditions:

with Ni/NiO-diatomite at 200; for 3 h;Autoclave;Inert atmosphere;Reagent/catalyst;

Steps:

5
200 m of 1,4-cyclohexane dimethanol (trans isomer 67%, cis isomer 33%) and 200 m of the catalyst shown in the following Table 1 were introduced into a 500 ml autoclave(Comparative Example 6 is no catalyst) And the mixture was stirred at 200°C For 3 hours in a nitrogen atmosphere.

References:

SK Chemicals Co., Ltd.;Kim, Tae Jung;Lee, Dong Ju KR2015/2258, 2015, A Location in patent:Paragraph 0058-0061

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