| Identification | Back Directory | [Name]
1-(2-HYDROXY-5-METHYLPHENYL)-2-PHENYLETHAN-1-ONE | [CAS]
24258-63-7 | [Synonyms]
2'-HYDROXY-5'-METHYL-2-PHENYLACETOPHENONE
Ethanone, 1-(2-hydroxy-5-methylphenyl)-2-phenyl-
1-(2-HYDROXY-5-METHYLPHENYL)-2-PHENYLETHAN-1-ONE | [Molecular Formula]
C15H14O2 | [MDL Number]
MFCD00082971 | [MOL File]
24258-63-7.mol | [Molecular Weight]
226.27 |
| Hazard Information | Back Directory | [Preparation]
Preparation by Fries rearrangement of p-cresyl phenylacetate with aluminium chloride (68%),
? without solvent at 120–140° for 20 min (82%) , at 130–135° for 30 min (80%) or at 130–140° for 3 h (14%);
? in nitrobenzene at r.t. for 48 h (80%) or at 60° for 4 h (64%) ;
? in 1,2,4-trichlorobenzene at reflux for 30 min (78%);
? in chlorobenzene at reflux for 4 h (23%) or for 30 min (86%). |
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