| Identification | Back Directory | [Name]
(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE | [CAS]
329944-59-4 | [Synonyms]
Methanone, (3-bromo-5-chlorophenyl)(5-chloro-2-methoxyphenyl)-
(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE | [Molecular Formula]
C14H9BrCl2O2 | [MDL Number]
MFCD09031573 | [MOL File]
329944-59-4.mol | [Molecular Weight]
360.03 |
| Hazard Information | Back Directory | [Preparation]
A solution of 1,3-dibromo-5-chlorobenzene (1 mmol) in ethyl ether was cooled to ?78° and n-butyllithium in hexane (1.1 mmol) was added over 2 min.The reaction mixture was stirred at ?78° for an additional 10 min, and then 5-chloro-N,2-dimethoxy-N-methylbenzamide (1 mmol) was added in small portions over 4 min. The reaction mixture was stirred at ?78° for 1.25 h and then allowed to warm to r.t. and stirred for 14 h (97%). |
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