| Chemical Properties | Back Directory | [Melting point ]
57°C | [Boiling point ]
174-178°C/3mm | [Fp ]
174-178°C/3mm | [storage temp. ]
2-8°C | [form ]
liquid | [color ]
white to yellow | [Water Solubility ]
Not miscible or difficult to mix in water. | [Sensitive ]
Moisture Sensitive |
| Hazard Information | Back Directory | [Purification Methods]
It is purified by fractional distillation in a vacuum (b 179-183o/7mm, 253-257o/15mm,) and the distillate solidifies (m 36o, also reported is m 37o). [Weinberg J Org chem. 40 3586 1975, McEwen et al. J Am Chem Soc 100 7304 1978, Beilstein 16 H 769, 16 IV 970 for chlorodi(p-tolyl)phosphine.] |
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