ChemicalBook--->CAS DataBase List--->60013-02-7

60013-02-7

60013-02-7 Structure

60013-02-7 Structure
IdentificationBack Directory
[Name]

3,4-Dichloro-4'-hydroxybenzophenone
[CAS]

60013-02-7
[Synonyms]

Fenofibrate impurity 5
Fenofibrate Impurity 14
3,4-Dichloro-4'-hydroxybenzophenone
3,4-dichlorophenyl 4-hydroxyphenyl ketone
(3,4-Dichlorophenyl)(4-hydroxyphenyl)methanone
Methanone, (3,4-dichlorophenyl)(4-hydroxyphenyl)-
[Molecular Formula]

C13H8Cl2O2
[MOL File]

60013-02-7.mol
[Molecular Weight]

267.11
Chemical PropertiesBack Directory
[Melting point ]

172-174 °C
[Boiling point ]

444.5±45.0 °C(Predicted)
[density ]

1.406±0.06 g/cm3(Predicted)
[pka]

7.50±0.15(Predicted)
Hazard InformationBack Directory
[Preparation]

Preparation by reaction of 3,4-dichlorobenzoyl chloride,
? with phenol in the presence of aluminium chloride;
? with phenetole in the presence of aluminium chloride in carbon disulfide at r.t. overnight (40%);
? with anisole in the presence of aluminium chloride at 70° for 4 h, followed by demethylation of the obtained ketone with 48% hydrobromic acid in refluxing acetic acid for 47 h.
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