Identification | Back Directory | [Name]
Ethanone, 2-fluoro-1-(4-methoxyphenyl)- (9CI) | [CAS]
73744-44-2 | [Synonyms]
2-fluoro-1-(4-methoxyphenyl)ethanone Ethanone, 2-fluoro-1-(4-methoxyphenyl)- Ethanone, 2-fluoro-1-(4-methoxyphenyl)- (9CI) | [Molecular Formula]
C9H9FO2 | [MOL File]
73744-44-2.mol | [Molecular Weight]
168.16 |
Hazard Information | Back Directory | [Preparation]
Obtained by reaction of fluoroacetyl chloride with anisole in the presence of aluminium chloride in chloroform at r.t. Also obtained by reaction of pyridinium poly(hydrogen fluoride) with 4-methoxy-a-diazo-acetophenone in ethyl ether at r.t. for 24 h (54%) Also obtained by reaction of Selectfluor with 1-(4-methoxyphenyl)ethanone in boiling methanol for 24 h (71%) Preparation by adding Rongalite to a solution of dichlorofluoromethyl 4-methoxyphenyl ketone in ethanol under nitrogen. Then, the solution was refluxing for 45 min (65%). |
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