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73744-44-2

73744-44-2 Structure

73744-44-2 Structure
IdentificationBack Directory
[Name]

Ethanone, 2-fluoro-1-(4-methoxyphenyl)- (9CI)
[CAS]

73744-44-2
[Synonyms]

2-fluoro-1-(4-methoxyphenyl)ethanone
Ethanone, 2-fluoro-1-(4-methoxyphenyl)-
Ethanone, 2-fluoro-1-(4-methoxyphenyl)- (9CI)
[Molecular Formula]

C9H9FO2
[MOL File]

73744-44-2.mol
[Molecular Weight]

168.16
Chemical PropertiesBack Directory
[Melting point ]

79-80 °C
[Boiling point ]

278.2±15.0 °C(Predicted)
[density ]

1.117±0.06 g/cm3(Predicted)
Hazard InformationBack Directory
[Preparation]

Obtained by reaction of fluoroacetyl chloride with anisole in the presence of aluminium chloride in chloroform at r.t.
Also obtained by reaction of pyridinium poly(hydrogen fluoride) with 4-methoxy-a-diazo-acetophenone in ethyl ether at r.t. for 24 h (54%)
Also obtained by reaction of Selectfluor with 1-(4-methoxyphenyl)ethanone in boiling methanol for 24 h (71%)
Preparation by adding Rongalite to a solution of dichlorofluoromethyl 4-methoxyphenyl ketone in ethanol under nitrogen. Then, the solution was refluxing for 45 min (65%).
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