1,3,5-TRIIODOBENZENE
- CAS No.
- 626-44-8
- Chemical Name:
- 1,3,5-TRIIODOBENZENE
- Synonyms
- 5-Triiodobenzene;2,4,6-Triiodobenzene;1,3,5-TRIIODOBENZENE;Benzene, 1,3,5-triiodo-;1,3,5-TRIIODOBENZENE, 95 %
- CBNumber:
- CB1294914
- Molecular Formula:
- C6H3I3
- Molecular Weight:
- 455.8
- MDL Number:
- MFCD02690052
- MOL File:
- 626-44-8.mol
- MSDS File:
- SDS
Melting point | 184.2°C |
---|---|
Boiling point | 381.91°C (rough estimate) |
Density | 2.8493 (rough estimate) |
refractive index | 1.8070 (estimate) |
storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
solubility | Chloroform (Slightly), Methanol (Slightly, Heated) |
form | Solid |
color | White to Off-White |
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H315-H319-H335 |
Precautionary statements | P261-P305+P351+P338 |
1,3,5-TRIIODOBENZENE price More Price(20)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Matrix Scientific | 097888 | 1,3,5-Triiodobenzene 95+% | 626-44-8 | 250mg | $59 | 2021-12-16 | Buy |
AK Scientific | J54628 | 1,3,5-Triiodobenzene | 626-44-8 | 250mg | $60 | 2021-12-16 | Buy |
Matrix Scientific | 097888 | 1,3,5-Triiodobenzene 95+% | 626-44-8 | 500mg | $91 | 2021-12-16 | Buy |
Ark Pharm | AK101088 | 1,3,5-Triiodobenzene 98% | 626-44-8 | 10g | $572 | 2021-12-16 | Buy |
American Custom Chemicals Corporation | HCH0295342 | 1,3,5-TRIIODOBENZENE 98.00% | 626-44-8 | 1G | $1270.5 | 2021-12-16 | Buy |
1,3,5-TRIIODOBENZENE Chemical Properties,Uses,Production
Uses
1,3,5-Triiodobenzene is used in the synthesis of conjugated microporous polymers through cationic cyclization polymerization. It also can be used in optical materials.
Synthesis
1,3,5-Triiodobenzene was synthesized by reacting 2,4,6-triiodoaniline with NaNO2 in the presence of copper(I) oxide.
Experimental procedure: Finely ground NaNO2 (1.95 g,
0.028 mol) was slowly added with stirring to sulfuric acid
(3.5 mL). Then a solution of 2,4,6-triiodoaniline(2.90 g,
6.16 mmol) in glacial AcOH (130 mL) was added dropwise with
stirring and cooling at such a rate that the temperature of the
reaction mixture was kept below 20 °C. Following addition of
the amine, the reaction mixture was stirred at ≈20 °C for about
30 min. The resulting solution of the diazonium salt was added
dropwise to a suspension of copper(I) oxide (2.52 g) in dry ethanol (70 mL) with vigorous stirring over 15 min. The reaction
mixture was brought to boiling and stirred for 30 min until
elimination of nitrogen ceased. Then the mixture was cooled,
kept for one day, poured into ice water (300 mL), and extracted
with benzene (3×50 mL). The benzene extracts were dried with
anhydrous Na2SO4 and the solvent was distilled off in vacuo.
The residue was repeatedly recrystallized from benzene. The
yield was 2.01 g (84%), m.p. 182 °C (cf. lit. data11: m.p. 183 °C).
1H NMR (CDCl3), δ: 8.02 (s, 3 H, CH). 13C NMR (CDCl3),
δ: 79; 128.
1,3,5-TRIIODOBENZENE Preparation Products And Raw materials
1,3,5-TRIIODOBENZENE Suppliers
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 | info@fdachem.com | China | 20260 | 58 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32965 | 60 |
Shaanxi Dideu Medichem Co. Ltd | +86-29-87569262 +86-15003564040 | 1087@dideu.com | China | 3167 | 58 |
Career Henan Chemica Co | +86-0371-86658258 +8613203830695 | laboratory@coreychem.com | China | 30233 | 58 |
CD Chemical Group Limited | +8615986615575 | info@codchem.com | China | 20342 | 58 |
LEAP CHEM CO., LTD. | +86-852-30606658 | market18@leapchem.com | China | 24727 | 58 |
Aromsyn Co., Ltd. | +86-0571-85585865 +8613336024896 | CB@aromsyn.com | China | 19183 | 58 |
Hebei Weibang Biotechnology Co., Ltd | +8617732866630 | bess@weibangbio.com | China | 18147 | 58 |
SUZHOU SENFEIDA CHEMICAL CO.,LTD | +86-0512-83500002 +8615195660023 | sales@senfeida.com | China | 23046 | 58 |
Shanghai Acmec Biochemical Technology Co., Ltd. | +86-18621343501; +undefined18621343501 | product@acmec-e.com | China | 33338 | 58 |
View Lastest Price from 1,3,5-TRIIODOBENZENE manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
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2023-12-29 | 1,3,5-TRIIODOBENZENE
626-44-8
|
US $101.00-1.00 / KG | 1KG | 99% | g-kg-tons, free sample is available | Henan Fengda Chemical Co., Ltd |
-
- 1,3,5-TRIIODOBENZENE
626-44-8
- US $101.00-1.00 / KG
- 99%
- Henan Fengda Chemical Co., Ltd