9-(3-Bromophenyl)-9-phenyl-9H-fluorene
- CAS No.
- 1257251-75-4
- Chemical Name:
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
- Synonyms
- 3-BPF;9-(3-Bromophenyl)-9-phenyl-fluorene;9-(3-bromophenyl)-9-phenyl-9H-fluoren;9-(3-Bromophenyl)-9-phenyl-9H-fluorene;9H-Fluorene, 9-(3-bromophenyl)-9-phenyl-;9-(3-Bromophenyl)-9-phenyl-9H-fluorene ISO 9001：2015 REACH
- CBNumber:
- CB13044385
- Molecular Formula:
- C25H17Br
- Molecular Weight:
- 397.31
- MDL Number:
- MFCD30187277
- MOL File:
- 1257251-75-4.mol
- MSDS File:
- SDS
| Melting point | 131.0 to 135.0 °C |
|---|---|
| Boiling point | 480.5±24.0 °C(Predicted) |
| Density | 1.363±0.06 g/cm3(Predicted) |
| solubility | soluble in Toluene |
| form | powder to crystal |
| color | White to Almost white |
| CAS DataBase Reference | 1257251-75-4 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 |
| HS Code | 2903.99.8001 |
9-(3-Bromophenyl)-9-phenyl-9H-fluorene price More Price(11)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TCI Chemical | B5616 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene >98.0%(GC) | 1257251-75-4 | 1g | $73 | 2024-03-01 | Buy |
| TCI Chemical | B5616 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene >98.0%(GC) | 1257251-75-4 | 5g | $221 | 2024-03-01 | Buy |
| TRC | B807928 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene | 1257251-75-4 | 50mg | $60 | 2021-12-16 | Buy |
| Arctom | AS009872 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene | 1257251-75-4 | 25g | $427 | 2021-12-16 | Buy |
| Alichem | 1257251754 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene | 1257251-75-4 | 100g | $499 | 2021-12-16 | Buy |
9-(3-Bromophenyl)-9-phenyl-9H-fluorene Chemical Properties,Uses,Production
Uses
9-(3-Bromophenyl)-9-phenyl-9H-fluorene is a useful research chemical.
Description
9-(3-Bromophenyl)-9-phenyl-9H-fluorene (9-(3-bromophenyl)-9-phenylfluorene) is an important organic intermediate to synthetize its substituted products.
Synthesis
A solution of 10.0 g of 2-bromobiphenyl (42.9 mmol) in 70 ml of anhydrous THF was added to a 500 mE 3-neck flask and cooled to -78 C. 27 ml of a 1.58 M hexane solution of n-BuEi (42.9 mmol) was then added dropwise while stirring, and the reaction was stirred for about 2.5 hours. A solution of 9.30 g (35.6 mmol) of 3-bromobenzophenone in 85 mE of an anhydrous THF was added dropwise, and the resulting mixture was stirred for about 2 hours at -78 C. followed by stirring for about 3 hours at room temperature. 1 N hydrochloric acid (HC1) was then added to the mixture and stirred for about 1 hour. The mixture was washed with water, and the resultant organic phase was concentrated to afford a material having a candy-like consistency. The candy-like material, 50 ml of acetic acid, and 2.4 ml of hydrochloric acid were added to a 500 mL recovery flask, and the mixture was stirred and reacted at 130 C. under a nitrogen atmosphere for about 2 hours. After the reaction, the reaction mixture was added dropwise to 350 ml of ice-cold water, precipitating white crystals, and the crystals were isolated by filtration. The crystals were washed with methanol and allowed to dry. About 13.3 g of Compound A was obtained as a white powder (yield: about 78%).
9-(3-Bromophenyl)-9-phenyl-9H-fluorene Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Hebei Xinsheng New Material Technology Co., LTD. | +86-16632316109 | xinshengkeji@xsmaterial.com | China | 1085 | 58 |
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 | info@fdachem.com | China | 20284 | 58 |
| Qingdao Xinli Technology Development Co., Ltd. | +8616632313095 | xinlikeji01@qdxlchem.com | China | 124 | 58 |
| Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 | info@spring-chem.com | China | 2068 | 57 |
| Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18751 | 58 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32957 | 60 |
| AB PharmaTech,LLC | 323-480-4688 | sales@acrospharmatech.com | United States | 989 | 55 |
| Beijing Green Guardee Technology Co., Ltd | 86-010-69706062 | sales2@greenguardee.com | CHINA | 650 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29880 | 58 |
| Zhengzhou HQ Material CO.,LTD. | +86-371-55919009 +8615225108189 | sale1@hqmat.com | China | 832 | 58 |
Related articles
- Preparation of 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene (9-(3-bromophenyl)-9-phenylfluorene) is an important organic intermediate to synthetize....
- Nov 8，2019
View Lastest Price from 9-(3-Bromophenyl)-9-phenyl-9H-fluorene manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2024-12-10 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
|
US $0.00 / KG | 1KG | 98% | 150KG /month | Shanghai Daken Advanced Materials Co.,Ltd | |
 |
2024-10-12 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
|
US $0.00-0.00 / kg | 1kg | 99% | 20 tons | Qingdao Xinli Technology Development Co., Ltd. | |
 |
2024-01-02 | 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
|
US $200.00-1.00 / KG | 1KG | 99%, 99.5% Sublimated | g-kg-tons, free sample is available | Henan Fengda Chemical Co., Ltd |
-
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
- US $0.00 / KG
- 98%
- Shanghai Daken Advanced Materials Co.,Ltd
-
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
- US $0.00-0.00 / kg
- 99%
- Qingdao Xinli Technology Development Co., Ltd.
-
- 9-(3-Bromophenyl)-9-phenyl-9H-fluorene
1257251-75-4
- US $200.00-1.00 / KG
- 99%, 99.5% Sublimated
- Henan Fengda Chemical Co., Ltd