ChemicalBook >> CAS DataBase List >>8-Methylene-1,4-dioxa-spiro[4.5]decane
8-Methylene-1,4-dioxa-spiro[4.5]decane
- CAS No.
- 51656-90-7
- Chemical Name:
- 8-Methylene-1,4-dioxa-spiro[4.5]decane
- Synonyms
- 8-METHYLENE-1,4-DIOXA-SPIRO[4.5]DECANE;8-METHYLENE-l, 4-DI0XASPIR0[4. 5]DECANE;1,4-Dioxaspiro[4.5]decane, 8-methylene-
- CBNumber:
- CB1767597
- Molecular Formula:
- C9H14O2
- Molecular Weight:
- 154.21
- MDL Number:
- MFCD07779440
- MOL File:
- Mol file
- MSDS File:
- SDS
Last updated:2023-11-28 14:26:34
Boiling point | 221.4±40.0 °C(Predicted) |
---|---|
Density | 1.04±0.1 g/cm3(Predicted) |
InChI | InChI=1S/C9H14O2/c1-8-2-4-9(5-3-8)10-6-7-11-9/h1-7H2 |
InChIKey | BCWKBPCNPHCCQS-UHFFFAOYSA-N |
SMILES | O1C2(CCC(=C)CC2)OCC1 |
CAS DataBase Reference | 51656-90-7 |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
---|---|
Signal word | Warning |
Hazard statements | H302 |
Precautionary statements | P280-P305+P351+P338 |
HS Code | 2932990090 |
8-Methylene-1,4-dioxa-spiro[4.5]decane price More Price(15)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
TRC | M223065 | 8-Methylene-1,4-dioxaspiro[4.5]decane | 51656-90-7 | 10mg | $45 | 2021-12-16 | Buy |
TRC | M223065 | 8-Methylene-1,4-dioxaspiro[4.5]decane | 51656-90-7 | 50mg | $175 | 2021-12-16 | Buy |
AK Scientific | 3099AL | 8-Methylene-1,4-dioxaspiro[4.5]decane | 51656-90-7 | 1g | $424 | 2021-12-16 | Buy |
Apolloscientific | OR451154 | 8-Methylene-1,4-dioxa-spiro[4.5]decane | 51656-90-7 | 1g | $501 | 2021-12-16 | Buy |
American Custom Chemicals Corporation | CHM0361777 | 8-METHYLENE-1,4-DIOXASPIRO[4.5]DECANE 95.00% | 51656-90-7 | 5MG | $504.16 | 2021-12-16 | Buy |
8-Methylene-1,4-dioxa-spiro[4.5]decane Chemical Properties,Uses,Production
Synthesis
Add BuLi to a solution of methyl triphenylphosphonium bromide in THF at -78° C. Stir this suspension for 10 min at -78° C, then 30 min at 0° C. Cool the orange solution obtained to -78° C, and add a solution of the monoethylene ketal of 1,4-cyclohexanedione in THF. Stir the reaction mixture overnight at room temperature (RT), then filter on Celite. Rinse the solid with pentane. After evaporating the solvents, the residue on the silica gel was chromatographed. 8-Methylene-1,4-dioxa-spiro[4.5]decane is thus obtained (colorless oil).
8-Methylene-1,4-dioxa-spiro[4.5]decane Preparation Products And Raw materials
Raw materials
Preparation Products
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8-METHYLENE-1,4-DIOXA-SPIRO[4.5]DECANE
1,4-Dioxaspiro[4.5]decane, 8-methylene-
8-METHYLENE-l, 4-DI0XASPIR0[4. 5]DECANE
51656-90-7
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