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4-Chloro-3-nitrobenzenesulfonamide

CAS No.
97-09-6
Chemical Name:
4-Chloro-3-nitrobenzenesulfonamide
Synonyms
4-chloro-3-nitrobenzenesulphonamide;YELLOW SULFONE;BUTTPARK 76\07-88;4-Chloro-3-Nitrosulfonamide;4-CHLORO-3-NITROSULFAMYLBENZENE;2-NITROCHLOROBENZENE-4-SULFONAMIDE;O-NITROCHLOROBENZENE-P-SULFONAMIDE;4-chloro-3-nitro-benzenesulfonamid;3-NITRO-4-CHLOROBENZENESULFONAMIDE;4-CHLORO-3-NITROBENZENESULFONAMIDE
CBNumber:
CB2243863
Molecular Formula:
C6H5ClN2O4S
Molecular Weight:
236.63
MDL Number:
MFCD00035783
MOL File:
97-09-6.mol
MSDS File:
SDS
Last updated:2024-08-15 19:00:21

4-Chloro-3-nitrobenzenesulfonamide Properties

Melting point 25-35 °C
Boiling point 175-176 °C
Density 1.5966 (rough estimate)
refractive index 1.6000 (estimate)
storage temp. Inert atmosphere,Room Temperature
form crystalline powder
pka 9.28±0.60(Predicted)
color White to off white
Water Solubility 224.8mg/L(15 ºC)
CAS DataBase Reference 97-09-6(CAS DataBase Reference)
FDA UNII 2O1T5ZXF22
EPA Substance Registry System Benzenesulfonamide, 4-chloro-3-nitro- (97-09-6)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P305+P351+P338
Hazard Codes  Xi
Hazard Note  Irritant
HS Code  2935909099

4-Chloro-3-nitrobenzenesulfonamide price More Price(23)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Apolloscientific OR24156 4-Chloro-3-nitrobenzenesulphonamide 97-09-6 5g $25 2021-12-16 Buy
SynQuest Laboratories 8669-5-X7 4-Chloro-3-nitrobenzene-1-sulfonamide 97-09-6 5G $28 2021-12-16 Buy
Matrix Scientific 098414 3-Nitro-4-chlorobenzenesulfonamide 95+% 97-09-6 5g $53 2021-12-16 Buy
Biosynth Carbosynth FC146441 4-Chloro-3-nitrobenzenesulfonamide 97-09-6 25g $80 2021-12-16 Buy
Apolloscientific OR24156 4-Chloro-3-nitrobenzenesulphonamide 97-09-6 25g $83 2021-12-16 Buy
Product number Packaging Price Buy
OR24156 5g $25 Buy
8669-5-X7 5G $28 Buy
098414 5g $53 Buy
FC146441 25g $80 Buy
OR24156 25g $83 Buy

4-Chloro-3-nitrobenzenesulfonamide Chemical Properties,Uses,Production

Chemical Properties

Light yellow to light brown crystalline powder

Uses

4-Chloro-3-nitrobenzenesulfonamide is used as a chemical intermediate for azo dyes.

Synthesis

Chlorosulphonic acid (450 mL) was slowly added to 2-chloronitrobenzene (100 g). The reaction mass was heated to 100°C and maintained at that temperat ure for 6 hours before cooling to ambient temperature and stirring for an additional 12 hours. The reaction mass was slowly poured into chilled aqueous ammonia (800 mL) and the reaction mixture was stirred for 3 hours at -10°C. The reaction mixture was then warmed to 23°C and stirred for 2 h ours. The reaction mixture was then filtered and the obtained solid was washed three times with water (200 mL x 3). The solid was dissolved in methanol (600 mL) at 60°C, charged with water (200 mL), and was stirred for 1 hour at 60°C. Again, the reaction mixture was charged with water (200 mL) and stirred for 1 hour at 60°C. Once again, the reaction mixtu re was charged with water (200 mL) and stirred for 1 hour. After cooling to room temperature and stirring for 1 hour, the reaction mixture was filtered, and the solid was washed with a 1 :1 mixture of methanol and water (100 mL). The solid was dried under vacuum at 60°C. Crystallization of the residue with toluen e gave the 4-Chloro-3-nitrobenzenesulfonamide(50 g).
97-09-6.png

Global( 191)Suppliers
Supplier Tel Email Country ProdList Advantage
Shaanxi Dideu Medichem Co. Ltd
+86-29-81148696 +86-15536356810 1022@dideu.com China 3882 58
Shanghai Daken Advanced Materials Co.,Ltd
+86-371-66670886 info@dakenam.com China 18751 58
career henan chemical co
+86-0371-86658258 +8613203830695 sales@coreychem.com China 29880 58
NINGBO INNO PHARMCHEM CO., LTD.
13867897135 sales@nbinno.com CHINA 923 58
Shenzhen Nexconn Pharmatechs Ltd
+86-755-89396905 +86-15013857715 admin@nexconn.com China 10311 58
Hubei Jusheng Technology Co.,Ltd.
18871490254 linda@hubeijusheng.com CHINA 28172 58
Hubei xin bonus chemical co. LTD
86-13657291602 linda@hubeijusheng.com CHINA 22963 58
Chongqing Chemdad Co., Ltd
+86-023-6139-8061 +86-86-13650506873 sales@chemdad.com China 39894 58
Alchem Pharmtech,Inc.
8485655694 sales@alchempharmtech.com United States 63687 58
CONIER CHEM AND PHARMA LIMITED
+8618523575427 sales@conier.com China 49374 58

View Lastest Price from 4-Chloro-3-nitrobenzenesulfonamide manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
4-Chloro-3-nitrobenzenesulfonamide pictures 2024-08-15 4-Chloro-3-nitrobenzenesulfonamide
97-09-6
US $0.00-0.00 / KG 1KG 99.0% 1000KG Shaanxi Dideu Medichem Co. Ltd
4-Chloro-3-nitrobenzenesulfonamide pictures 2019-07-06 4-Chloro-3-nitrobenzenesulfonamide
97-09-6
US $1.00 / kg 1kg 99% 200kg Career Henan Chemical Co

4-Chloro-3-nitrobenzenesulfonamide Spectrum

BUTTPARK 76\07-88 3-NITRO-4-CHLOROBENZENESULFONAMIDE 4-CHLORO-3-NITROBENZENE-1-SULFONAMIDE 4-CHLORO-3-NITROBENZENESULFONAMIDE 4-CHLORO-3-NITROSULFAMYLBENZENE YELLOW SULFONE 4-chloro-3-nitro-benzenesulfonamid O-NITROCHLOROBENZENE-P-SULFONAMIDE 2-NITROCHLOROBENZENE-4-SULFONAMIDE 4-Chloro-3-nitrobenzene-1-sulphonamide 3-Nitro-4-chlorobenzensulfonyl amine 4-Chloro-3-Nitrosulfonamide Benzenesulfonamide, 4-chloro-3-nitro- 4-chloro-3-nitrobenzenesulphonamide 97-09-6 1997-09-6 1997-9-6 C6H5ClN2O4S ClC6H3NO2SO2NH2 C6H3ClNO5S Benzene derivates Intermediates of Dyes and Pigments