[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid
- CAS No.
- 446299-81-6
- Chemical Name:
- [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid
- Synonyms
- OzoxacinIntermediateD;Ozenoxacin Impurity 7;Ozenoxacin Impurity 15;5-Methyl-6-(phenacylamino)pyridin-3-yl]boronic acid;(5-methyl-6-(N-methylbenzamido)pyridin-3-yl)boronic acid;[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid;[6- [benzoyl (methyl) amino] -5-methyl-3-pyridinyl] boric acid;(5-methyl-6-((2-oxo-2-phenylethyl)amino)pyridin-3-yl)boronic acid;Boronic acid, [6-(benzoylmethylamino)-5-methyl-3-pyridinyl]- (9CI);(S) - 6-chloro-3,4-dihydro-2h-thieno [3,2-e] - 1,2-thiazine-4-alcohol 1,1-dioxide
- CBNumber:
- CB23370678
- Molecular Formula:
- C14H15BN2O3
- Molecular Weight:
- 270.09
- MDL Number:
- MFCD32012267
- MOL File:
- 446299-81-6.mol
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() ![]() GHS07,GHS09 |
---|---|
Signal word | Warning |
Hazard statements | H317-H411 |
Precautionary statements | P261-P272-P280-P302+P352-P333+P313-P321-P363-P501 |
[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid Chemical Properties,Uses,Production
Uses
[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
Synthesis
Under a nitrogen atmosphere, N-(5-bromo-3-methyl-2-pyridinyl)-N-methylbenzamide 30.0 g was dissolved in 150 mL of tetrahydrofuran, triisopropyl borate 22.0 g was added. The reaction mixture was colled to-60 .DEGREE CELSIUS., n-butyl lithium (1.56 mol/L n-hexane solution) 69 mL was added dropwise required to between 20 minutes, and the mixture was stirred for 15 minutes at the same temperature.After raising the temperature of the reaction mixture at-20 .DEGREE CELSIUS., 390 mL of water was added dropwise, it was stirred for 30 min at room temperature,the aqueous layer was separated. The aqueous layer was fractionated and HCl 1 mol/L was added to adjust the pH at 4.5,the precipitate was collected by filtration, 6-[benzoyl(methyl)amino]-5-methyl-3-pyridinylboric acid 18.5 g was obtained as colorless solid.
[6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Hebei Xinsheng New Material Technology Co., LTD. | +86-16632316109 | xinshengkeji@xsmaterial.com | China | 1085 | 58 |
Hebei Junhua Import and Export Co., LTD | +86-18503288844 +86-18503288844 | junhua1@hb-junhua.com | China | 978 | 58 |
Jinan Chenghui-Shuangda Chemical Co.,Ltd | +86-531-58897082 | ericqiao@jnchsd.com | CHINA | 158 | 58 |
career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29808 | 58 |
Chengdu Aslee Biopharmaceuticals, Inc. | 28-85305008 | CHINA | 964 | 58 | |
Hebei Yanxi Chemical Co., Ltd. | +8617531153977 | allison@yan-xi.com | China | 5854 | 58 |
Hebei Miaobian Biotechnology Co., Ltd | +8617733850068 | CHINA | 967 | 58 | |
Hubei Ipure Biology Co., Ltd | +8613367258412 | ada@ipurechemical.com | China | 10244 | 58 |
ANHUI WITOP BIOTECH CO., LTD | +8615255079626 | eric@witopchemical.com | China | 23541 | 58 |
Baoji Guokang Healthchem co.,ltd | +8615604608665 15604608665 | dominicguo@gk-bio.com | CHINA | 9414 | 58 |
View Lastest Price from [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
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2025-04-27 | [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid
446299-81-6
|
US $0.00 / kg | 1kg | 98% | 1000 | Hebei Junhua Import and Export Co., LTD | |
![]() |
2025-04-27 | (S) - 6-chloro-3,4-dihydro-2h-thieno [3,2-e] - 1,2-thiazine-4-alcohol 1,1-dioxide
446299-81-6
|
US $0.00-0.00 / kg | 1kg | 0.99 | 800kg | Wuhan Biocar Pharmacy CO.,Ltd. | |
![]() |
2025-03-07 | (5-methyl-6-(N-methylbenzamido)pyridin-3-yl)boronic acid
446299-81-6
|
US $0.00 / kg | 1kg | 0.99 | 1000kg | Hebei Yanxi Chemical Co., Ltd. |
-
- [6-[benzoyl(methyl)amino]-5-methyl-3-pyridyl]boronic acid
446299-81-6
- US $0.00 / kg
- 98%
- Hebei Junhua Import and Export Co., LTD
-
- (S) - 6-chloro-3,4-dihydro-2h-thieno [3,2-e] - 1,2-thiazine-4-alcohol 1,1-dioxide
446299-81-6
- US $0.00-0.00 / kg
- 0.99
- Wuhan Biocar Pharmacy CO.,Ltd.
-
- (5-methyl-6-(N-methylbenzamido)pyridin-3-yl)boronic acid
446299-81-6
- US $0.00 / kg
- 0.99
- Hebei Yanxi Chemical Co., Ltd.