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3,5-Dibromosalicylaldehyde

3,5-Dibromosalicylaldehyde structure

CAS No.: 90-59-5

Chemical Name:: 3,5-Dibromosalicylaldehyde

Synonyms: Dalyde;AKOS B028985;AKOS BBS-00003256;OTAVA-BB BB7018801957;SALOR-INT L497649-1EA;LABOTEST-BB LT00137784;DibroMosalicylaldehyde;5-DibroMosalicylaldehyde;Dembrexine EP Impurity C;3,5-DIBROMOSALICYLADEHYDE

CBNumber:: CB2343352

Molecular Formula:: C7H4Br2O2

Molecular Weight:: 279.91

MDL Number:: MFCD00003318

MOL File:: 90-59-5.mol

MSDS File:: SDS

Last updated:2024-11-26 17:46:08

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3,5-Dibromosalicylaldehyde Properties

Melting point	82-83.5 °C (lit.)
Boiling point	261.2±35.0 °C(Predicted)
Density	1.9661 (rough estimate)
refractive index	1.4970 (estimate)
storage temp.	Keep in dark place,Sealed in dry,Room Temperature
solubility	methanol: soluble25mg/mL, clear, yellow to brown
form	Crystalline Powder
pka	6.08±0.23(Predicted)
color	Yellow to yellow-brown
Water Solubility	Soluble in methanol 25 mg/mL. Insoluble in water.
Sensitive	Air Sensitive
Merck	14,3027
BRN	1424739
InChIKey	JHZOXYGFQMROFJ-UHFFFAOYSA-N
CAS DataBase Reference	90-59-5(CAS DataBase Reference)
EWG's Food Scores	1
FDA UNII	7A260PBI3A
NIST Chemistry Reference	3,5-Dibromosalicylaldehyde(90-59-5)
EPA Substance Registry System	Benzaldehyde, 3,5-dibromo-2-hydroxy- (90-59-5)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07,GHS09

Signal word

Warning

Hazard statements

H315-H319-H335-H400

Precautionary statements

P273-P302+P352-P305+P351+P338

Hazard Codes

Risk Statements

36/37/38

Safety Statements

26-37/39-24/25

RIDADR

UN 3077 9 / PGIII

WGK Germany

RTECS

CU5609000

HazardClass

PackingGroup

III

HS Code

29130000

NFPA 704

	1
2		0

3,5-Dibromosalicylaldehyde price More Price(31)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	122130	3,5-Dibromosalicylaldehyde 98%	90-59-5	10g	$86.8	2024-03-01	Buy
TCI Chemical	D0188	3,5-Dibromosalicylaldehyde >98.0%(HPLC)(T)	90-59-5	5g	$38	2024-03-01	Buy
TCI Chemical	D0188	3,5-Dibromosalicylaldehyde >98.0%(HPLC)(T)	90-59-5	25g	$150	2024-03-01	Buy
Alfa Aesar	A13729	3,5-Dibromosalicylaldehyde, 98%	90-59-5	10g	$58.65	2024-03-01	Buy
Alfa Aesar	A13729	3,5-Dibromosalicylaldehyde, 98%	90-59-5	50g	$219.65	2024-03-01	Buy

Product number	Packaging	Price	Buy
122130	10g	$86.8	Buy
D0188	5g	$38	Buy
D0188	25g	$150	Buy
A13729	10g	$58.65	Buy
A13729	50g	$219.65	Buy

3,5-Dibromosalicylaldehyde Chemical Properties,Uses,Production

Chemical Properties

yellow to yellow-brown crystalline powder.
3,5-Dibromosalicylaldehyde has an aromatic odor, and like salicylaldehyde, the compound colors the skin bright yellow. It is readily soluble in ether, benzene, chloroform, and hot alcohol. It imparts a yellow colour to cold water and is slightly soluble in boiling water, so it may be purified by distillation with steam. With the addition of sodium hydroxide, the brilliant yellow sodium salt separates; it is difficultly soluble in cold water or alcohol but more readily soluble when heated with these solvents.

Uses

3,5-Dibromosalicylaldehyde reacts with alkyl cyanoacetates in the presence of ammonium acetate to yield 4H- chromenes. It can be used in the synthesis of Schiff base and can be used as reactant for synthesis of Schiff base ligands which forms mononuclear complexes with copper(II), nickel(II), zinc(II) and cobalt(II).

General Description

3,5-Dibromosalicylaldehyde reacts with alkyl cyanoacetates in the presence of ammonium acetate to yield 4H- chromenes.

Synthesis

3,5-Dibromosalicylaldehyde was obtained in nearly quantitative yield by dissolving 20 g. of salicylaldehyde in 100 cc. of glacial acetic acid, and adding a solution of 20 cc in small portions. of bromine in 100 cc. of glacial acetic acid[1].

References

[1] Brewster, C. M. “SCHIFF’S BASES FROM 3,5-DIBROMO-SALICYLALDEHYDE.” Journal of the American Chemical Society 46 11 (1924): 2463–2468.

3,5-Dibromosalicylaldehyde Preparation Products And Raw materials

Raw materials

5-Bromosalicylaldehyde

Preparation Products

3,5-DIBROMO-2-METHOXYBENZALDEHYDE 3,5-DIBROMO-2-ETHOXYBENZALDEHYDE 6,8-DIBROMO-2H-CHROMENE-3-CARBALDEHYDE 2-(BENZYLOXY)-3,5-DIBROMOBENZALDEHYDE 3,5-DibroMobenzene-1,2-diol

Ethyl 5,7-Dibromo-1-Benzofuran-2-Carboxylate 2-(2-AMINO-6,8-DIBROMO-3-CYANO-4H-CHROMEN-4-YL)MALONONITRILE 2H-1-Benzopyran-3-carboxylic acid, 6,8-dibromo-2-(trifluoromethyl)- 6,8-DibroMo-3-acetylcouMarin 2,4-DIBROMO-6-([(4-FLUOROPHENYL)IMINO]METHYL)BENZENOL

3,5-DIBROMOSALICYLALDOXIME

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3,5-Dibromosalicylaldehyde Suppliers

Global( 250)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Hubei Lidu New Material Technology Co., Ltd	+undefined+86-19307248857	liduxcl@163.com	China	1134	58
Hebei Weibang Biotechnology Co., Ltd	+8615531157085	abby@weibangbio.com	China	8810	58
Hebei Chuanghai Biotechnology Co,.LTD	+86-13131129325	sales1@chuanghaibio.com	China	5892	58
Qingdao RENAS Polymer Material Co., Ltd.	+86-0532-86867058 +86-18562606086	sales@qdrenas.com	China	476	58
Capot Chemical Co.,Ltd.	+86-（0）57185586718 +86-13336195806	sales@capot.com	China	29791	60
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	18775	58
Standardpharm Co. Ltd.	86-714-3992388	overseasales1@yongstandards.com	United States	14332	58
Changzhou Carman Chemical Co., Ltd.	15061933924		CHINA	514	58
CONIER CHEM AND PHARMA LIMITED	+8618523575427	sales@conier.com	China	49374	58
career henan chemical co	+86-0371-86658258 +8613203830695	factory@coreychem.com	China	29811	58

Supplier	Advantage
Hubei Lidu New Material Technology Co., Ltd	58
Hebei Weibang Biotechnology Co., Ltd	58
Hebei Chuanghai Biotechnology Co,.LTD	58
Qingdao RENAS Polymer Material Co., Ltd.	58
Capot Chemical Co.,Ltd.	60
Shanghai Daken Advanced Materials Co.,Ltd	58
Standardpharm Co. Ltd.	58
Changzhou Carman Chemical Co., Ltd.	58
CONIER CHEM AND PHARMA LIMITED	58
career henan chemical co	58

View Lastest Price from 3,5-Dibromosalicylaldehyde manufacturers

Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
2024-11-28	3,5-DIBROMOSALICYLALDEHYDE 90-59-5	US $0.00 / g	1g	98%	20tons	Hubei Lidu New Material Technology Co., Ltd
2024-11-26	3,5-Dibromosalicylaldehyde 90-59-5	US $0.00-0.00 / KG	1KG	99%	20 mt	Hebei Weibang Biotechnology Co., Ltd
2024-11-05	3,5-Dibromosalicylaldehyde 90-59-5	US $0.00-0.00 / g	10mg	99%HPLC	2000tons	Shaanxi Dideu Medichem Co. Ltd

3,5-DIBROMOSALICYLALDEHYDE
90-59-5
US $0.00 / g
98%
Hubei Lidu New Material Technology Co., Ltd

3,5-Dibromosalicylaldehyde
90-59-5
US $0.00-0.00 / KG
99%
Hebei Weibang Biotechnology Co., Ltd

3,5-Dibromosalicylaldehyde
90-59-5
US $0.00-0.00 / g
99%HPLC
Shaanxi Dideu Medichem Co. Ltd

3,5-Dibromosalicylaldehyde Spectrum

3,5-Dibromosalicylaldehyde(90-59-5)MS 3,5-Dibromosalicylaldehyde(90-59-5)¹HNMR 3,5-Dibromosalicylaldehyde(90-59-5)¹³CNMR 3,5-Dibromosalicylaldehyde(90-59-5)IR1 3,5-Dibromosalicylaldehyde(90-59-5)IR2 3,5-Dibromosalicylaldehyde(90-59-5)Raman

90-59-5(3,5-Dibromosalicylaldehyde)Related Search:

Salicylaldoxime Salicylaldehyde 5-Bromosalicylaldehyde METHYL 3,5-DIBROMO-2,4-DIMETHOXY-6-METHYLBENZOATE METHYL 3,5-DIBROMO-2-HYDROXYBENZOATE

3,5,4'-TRIBROMOSALICYLANILIDE METHYL 3,5-DIBROMO-2,4-DIHYDROXY-6-METHYLBENZOATE 3',5'-Dibromo-2'-hydroxyacetophenone 3,5-Dibromosalicylic acid ETHYL 3,5-DIBROMO-2,4-DIHYDROXY-6-METHYLBENZOATE

3,5-Dibromosalicylaldehyde oxime 3,5-Dibromobenzaldehyde 3,5-DIBROMO-2,4-DIHYDROXYBENZALDEHYDE 6,8-DIBROMO-3-FORMYLCHROMONE, 99% METHYL 3,5-DIBROMO-2-METHOXYBENZOATE

3,5-DIBROMOSALICYLAMIDE Flusalan 4'-CHLORO-6,8-DIBROMOFLAVONE

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LABOTEST-BB LT00137784 3,5-DIBROMO-2-HYDROXYBENZALDEHYDE 3,5-DIBROMOSALICYLADEHYDE 3,5-DIBROMOSALICYLALDEHYDE 3,5-DIBROMOSILICYLALDEHYDE SALOR-INT L497649-1EA OTAVA-BB BB7018801957 AKOS BBS-00003256 AKOS B028985 2-Hydroxy-3,5-dibromobenzaldehyde 3,5-dibromo-2-hydroxy-benzaldehyd 3,5-Dibromosalicylaldeyde Benzaldehyde, 3,5-dibromo-2-hydroxy- Dalyde Salicylaldehyde, 3,5-dibromo- 3,5-Dibromosalicylaldehyde,98% 5-DibroMosalicylaldehyde 3,5-dibroMo salicyclic aldehyde DibroMosalicylaldehyde 3,5- twochlorine salicylicaldehyde 3,5-Dibromosalicylaldehyde 98% 2-[[4-(dipropylsulfamoyl)phenyl]-oxomethoxy]benzoic acid Dembrexine EP Impurity C Dembrexine Impurity 3（Dembrexine EP Impurity C） 3,5-Dibromosalicylaldehyde > Dembrexine Hydrochloride Monohydrate EP Impurity C 90-59-5 Br2C6H2OHCHO Br2C6H22OHCHO Organic Building Blocks ALDEHYDE Carbonyl Compounds C7 Building Blocks Aldehydes Aldehydes C7 Carbonyl Compounds Aromatic Aldehydes & Derivatives (substituted) Benzaldehyde Adehydes, Acetals & Ketones Bromine Compounds Phenols